Inductively Coupled Plasma Mass Spectrometer

The DLSU Spectroscopy Laboratory is a full-service laboratory of the Central Instrumentation Facility under the Office of the Vice-Chancellor for Research and Innovation. One of the instruments that the laboratory operates is the Shimadzu Inductively Coupled Plasma Mass Spectrometer – 2030LF (ICPMS – 2030LF). The instrument is located in Room 205A Dr. George S. K. Ty Central Instrumentation Facility at DLSU Laguna Campus in Binan, Laguna.

The facility offers Analytical Services using ICP MS and accepts samples not only from DLSU researchers but also from outside clients (academe, government, and industry) for a fee (please see the schedule of fees).

Shimadzu ICPMS-2030 LF:

• Plasma ion source: Sample spray chamber: Cyclone chamber (electronically cooled)
• Plasma Torch: Mini torch
• Nebulizer: Coaxial
• High-frequency power supply unit: 27 MHz, max. 1.4 kW
• Mass spectrometer unit: Quadrupole mass spectrometer
• Mass number range: 5 to 260 mass number range, octopole collision cell
• Equipped with AS-10 Autosampler which allows multiple samples to be analyzed successively

Available Measurement Mode:

1. Qualitative Analysis
2. Quantitative Analysis

The DLSU Spectroscopy Laboratory offers the following services:

• Simultaneous trace level analysis of multiple elements
• Environmental, Drinking Water, and Wastewater Analysis

ICP MS analysis is charged per sample. Standards are charged as individual samples each. The fees are inclusive of sample analysis only. Reagents, standards, solvents, and sample preparation must be provided/shouldered/performed by the client.

ICP MS Analysis Rates
Please refer to the Spectroscopy Lab homepage for rates.

1. It is recommended that solid samples must undergo microwave-assisted digestion using ultrapure acids to prevent contamination.
2. Ensure that all the apparatus used for sample preparation are clean and free from contaminants. Once the samples are properly prepared, filter the samples to remove other particulates.
3. Label the samples properly and wrap them securely to prevent them from spilling. Wrap light-sensitive samples in aluminum foil or place them in amber bottles.
4. For samples requiring a specific temperature for storage, ensure to store them in iceboxes and label them with temperature requirements and add a “fragile” mark when necessary.
5. Pack the samples carefully for transport.
6. Submit the sample to DLSU for analysis.

STEP 1. Send your inquiries to [email protected], indicate your name and institution.

STEP 2. Once the discussion has been finalized, the ICP-MS Analysis Form will be sent out to the email address you used or you may download the form here. Kindly fill out the form completely with all the details (one form for EACH SAMPLE) and send photos of each sample. INCOMPLETE FORMS WILL NOT BE PROCESSED. Carefully read the Terms and Conditions indicated on the sample analysis form. For questions regarding the form, send an email to [email protected].

STEP 3. Prepare the samples. Ensure that the requirements for the preparation of samples for FTIR analysis are met.

STEP 4. Submit the analysis form together with the sample. Alternatively, electronic submission of forms can be accommodated through email.

STEP 5. A confirmation email will be sent to you once the form(s) have been received and checked. A quotation will be sent to you depending on the number of samples.

STEP 6. Once the form has been received, a quotation will be sent to you based on the number of samples and analysis you indicated in the UV-Vis Analysis form.

STEP 7. Once payment has been confirmed, CIF staff will provide you with information on how to send the samples to the lab.
NOTE: Samples will NOT BE PROCESSED UNLESS COMPLETE PAYMENT IS CONFIRMED.

STEP 8. Analyses results will be sent via email. Data and samples will be kept as stated in the analysis form.

Can I observe during the analysis?
Laboratory visits are restricted.

Do you offer rush analysis?

Yes. Rush analysis is available for twice the published rate. Please contact us for rush analysis at [email protected]

Do you provide a formatted analysis report with registered chemist signatures? 

Yes, we do at an ADDITIONAL FEE of Php 1,500.00 per sample. 

What is the average turnaround time (TAT)  for  UV-Vis analysis? 

The turnaround time is 2 weeks, depending on the number of samples and the volume of job orders in the laboratory. 

Do you accept purchase order  (PO), job order (JO), work order (WO) terms of payment? 

NO, we do not accept PO, JO, or WO payment terms. At the moment, ONLY cash or cheque deposits are accepted. 

Do you accommodate and test samples on weekends and holidays? 

NO, we do not accept samples during weekends or holidays. Operating days are Monday to Friday (8:00 AM to 5:00 PM).

If your contact information is not working, is there an alternative email?

Contact us at these alternative emails: [email protected]; [email protected]

ICPMS Analysis Form (doc)

DLSU Spectroscopy Laboratory
Central Instrumentation Facility
105 George S.K. Ty (GT) Building
De La Salle University Laguna Campus
Laguna Boulevard, LTI Spine Road, Barangays Biñan and Malamig, Binan, Laguna

e-mail: [email protected]